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Journal of Nanchang University(Natural Science). 2015, (04) Core

Microwave assisted synthesis of 8-HydroxyquinolineChinese Full Text

YANG Jinyuan;SUO Zili;CHEN Qian;LIANG Juan;HE Laihua;ZHANG Yi;LU Xiaolan;College of Chemistry,Nanchang University;College of Resources,Environmental and Chemical Engineering,Nanchang University;College of Pharmacy,Nanchang University;

Abstract: 8-ydroxyquinoline was synthesized by the Skraup reactions,using o-nitrophenol,o-aminophenol and glycerol as materials,with concentrated sulfuric acid as the catalyst,as well as the assistance of microwave radiation.The optimized reaction conditions were as followings:（1）n（o-aminophenol）:n（o-nitrophenol）:n（concentrated sulfuric acid）:n（glycerol）=10.52.35;（2）the microwave power was 500 W;（3）the reaction temperature was 160℃;and（4）the reaction time was 40 minutes.Under these optimizing condition... More
Keywords：

microwave synthesis; 8-Hydroxyquinoline; Skraup reaction;

  • DOI：

    10.13764/j.cnki.ncdl.2015.04.016

  • Series：

    (A) Mathematics/ Physics/ Mechanics/ Astronomy; (B) Chemistry/ Metallurgy/ Environment/ Mine Industry

  • Subject：

    Chemistry

  • Classification Code：

    O626

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